山西大学学报（自然科学版）2013，Vol.36Issue(2)：245-248,4.
一种桥连β-二亚胺的合成及结构表征
Synthesis and Structural Characterization of a Bridged β-Diketiminate Compound
摘要
Abstract
A novel bridged β-diketiminate compound was synthesized by the reaction of bis-Schiff base compound and cyanobenzene including a 1,3-shift of trimethylsilyl from C atom to N atom.The compound was characterized by 1H NMR,13C NMR,elemental analysis and X-ray single crystal diffraction.The crystal of the title compound belongs to triclinic P-1 space group,with a =6.335 (7) (A),b =10.447 (14) (A),c =14.227(9)(A);α =71.53°,β =82.90°,γ=83.34°,V =883.2(16)(A)3,Z =1.关键词
有机合成/桥连β-二亚胺/配体Key words
organic synthesis/ bridged β-Diketiminato/ ligand分类
化学化工引用本文复制引用
张伟,张宇浩,姚吉祥,郭志强,魏学红..一种桥连β-二亚胺的合成及结构表征[J].山西大学学报（自然科学版）,2013,36(2):245-248,4.基金项目
山西省自然科学基金(2008011021 （）
2008012013-2) （）
山西省回国留学基金 （）
