中国粉体技术2013，Vol.19Issue(3)：39-42,4.DOI:10.3969/j.issn.1008-5548.2013.03.010
高能球磨技术制备Fe78-xMxSi13B9磁性材料
Preparation of Fe78-xMxSi13B9 Magnetic Materials by High-energy Ball-milling Technology
摘要
Abstract
Fe78-xMxSi13B9 soft magnetic amorphous alloy powders were prepared by high-energy ball-milling technology.Effects of the addition of transition metal elements M (Zr,Nb and Mo) on microstructure evolution,thermal stability and soft magnetic properties were analyzed by XRD,DSC,SEM and VSM.The results show that the addition of Zr and Nb are helpful to form amorphous phase in Fe-Si-B alloys.The maximum supercooled liquid region ΔTx is 70.62 K.The glass transition temperature Tgand the crystallization temperature Tx are respectively 785.05 and 855.67 K.The saturation magnetization Ms is 111 emu/g and the coercive force Hc is about 2 028.443 A/m.关键词
高能球磨/软磁非晶合金/饱和磁化强度Key words
high-energy ball-milling/ soft magnetic amorphous alloy/saturation magnetization分类
矿业与冶金引用本文复制引用
王兴华,王葛,王海舰,朱玉英,李强..高能球磨技术制备Fe78-xMxSi13B9磁性材料[J].中国粉体技术,2013,19(3):39-42,4.基金项目
河北省应用基础研究计划重点基础研究项目,编号:13961001D （）
国家重点基础研究发展计划(973计划)前期研究专项,编号:2009CB626603. （973计划）
