应用化学2013，Vol.30Issue(6)：623-627,5.DOI:10.3724/SP.J.1095.2013.20368
微波辐射硝基芴与丙烯酸酯Michael加成产物的合成与结构
Microwave-assisted Michael Additions Between Nitrofluorene and Acrylic Esters
摘要
Abstract
Using nitrofluorene and acrylic esters as precursors,a series of Michael addition products with high yields of 79％ ～87％ was obtained under microwave irradiation(500 W) for 4 ～ 5 min in the presence of sodium hydroxide.The strcutures of products were characterized by IR,1H NMR,MS and elemental analysis.The crystal structure of compound 3b was determined by single X-ray diffraction analysis.关键词
硝基芴/Michael加成/微波合成Key words
nitrofluorene/ Michael addition/microwave-assisted分类
化学化工引用本文复制引用
胡卫兵,黄猛,冯驸,崔治财,刘信平..微波辐射硝基芴与丙烯酸酯Michael加成产物的合成与结构[J].应用化学,2013,30(6):623-627,5.基金项目
湖北省自然科学基金资助项目(2012FFB01103) （2012FFB01103）
