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环氧树脂聚酰胺体系微波固化特性研究

耿杰 李勇 陈云雷 肖军 周克印

玻璃钢/复合材料Issue(5):7-13,7.
玻璃钢/复合材料Issue(5):7-13,7.

环氧树脂聚酰胺体系微波固化特性研究

STUDY ON CURING BEHAVIOR OF EPOXY POLYAMIDE MICROWAVE CURING SYSTEM

耿杰 1李勇 1陈云雷 1肖军 1周克印2

作者信息

  • 1. 南京航空航天大学材料科学与技术学院,南京 210016
  • 折叠

摘要

Abstract

Compared with traditional heat curing,microwave curing has the advantages of high efficiency,nonpollution,low cost of equipment and so on.As known,curing degree is determined by DSC,which is used to describe the progress of the microwave curing behavior of bisphenol-A type epoxy resin E51/650 polyamide reaction system.According to the curing efficiency,this paper optimizes formula ratio of the system component.Then,an orthogonal experiment table was designed to investigate microwave curing process parameters and contrast glass-transition temperatures of cured products in two different curing methods.The results showed that the optimal proportion of the system for microwave curing is 100 to 80 to 12 ratio of epoxy E51 to 650 polyamide to 660 A active diluents.And the order of microwave curing parameters that affect the degree of cure is the heating time,the output power,heating cycle and intermittent time.In addition,the glass-transition temperature and bending property of microwave curing product is decreased at a certain extent that because of the uniformity of microwave field and the output way of microwave power.

关键词

微波固化/环氧树脂/工艺参数/玻璃化转变温度

Key words

microwave curing / epoxy resin / technological parameter/ glass-transition temperature

分类

通用工业技术

引用本文复制引用

耿杰,李勇,陈云雷,肖军,周克印..环氧树脂聚酰胺体系微波固化特性研究[J].玻璃钢/复合材料,2013,(5):7-13,7.

基金项目

国家科技支撑计划(2012BAA01B02) (2012BAA01B02)

玻璃钢/复合材料

OA北大核心CSCDCSTPCD

2096-8000

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