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采用石墨电极制备多孔硅工艺研究

李进 庞骏敏 高忙忙 梁森 王晓芳 薛子文

硅酸盐通报2013,Vol.32Issue(7):1394-1396,3.
硅酸盐通报2013,Vol.32Issue(7):1394-1396,3.

采用石墨电极制备多孔硅工艺研究

Study on Porous Silicon Prepared by Using Graphite Electrode

李进 1庞骏敏 1高忙忙 1梁森 1王晓芳 1薛子文1

作者信息

  • 1. 宁夏大学宁夏光伏材料重点实验室,银川750021
  • 折叠

摘要

Abstract

By using graphite electrode as cathode and adding some nitric acid (HNO3,65%) into corrosion solution mixed by 40% hydrofluoric acid (HF) and 99.7% ethanol absolute (C2HsOH),porous silicon can be prepared by electrochemical method on monocrystalline silicon wafers.The results showed that contour root-mean-square deviation and average diameter of grain of porous silicon present periodic change,under the corrosive factors of 10 mA/cm2 and 1875 seconds,the above indicators of porous silicon are much bigger.The analysis of AFM and SEM showed that the maximum height,the maximum diameter and average diameter of silicon pillars achieved 470 nm,1693.590 nm and 489.954 nm respectively.

关键词

石墨电极/多孔硅/轮廓均方根偏差/颗粒平均直径/电化学方法/碳原子剥离

Key words

graphite electrode / porous silicon/ contour root-mean-square deviation/ electrochemical methods/ peel of carbon atoms

分类

信息技术与安全科学

引用本文复制引用

李进,庞骏敏,高忙忙,梁森,王晓芳,薛子文..采用石墨电极制备多孔硅工艺研究[J].硅酸盐通报,2013,32(7):1394-1396,3.

基金项目

宁夏自治区2012科技支撑计划项目 ()

硅酸盐通报

OA北大核心CSCDCSTPCD

1001-1625

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