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凝胶燃烧法制备镍掺杂氧化锌及其光致发光性能

陈建华 程好 赵俊锋

Journal of Changshu Institute of TechnologyIssue(4):6-9,4.
Journal of Changshu Institute of TechnologyIssue(4):6-9,4.

凝胶燃烧法制备镍掺杂氧化锌及其光致发光性能

Zn1-xNixO Prepared by Sol-gel Auto-combustion Method and Its Optical Photoluminescence

陈建华 1程好 2赵俊锋1

作者信息

  • 1. 常熟理工学院化学与材料工程学院,江苏常熟215500
  • 2. 南京工业大学材料科学与工程学院,南京210009
  • 折叠

摘要

Abstract

  Zn1-xNixO (x=0, 0.01, 0.02, 0.03, 0.04) nano-powders about 100nm to 300nm are prepared by sol-gel au⁃to-combustion method. Structural and optical properties of the samples are characterized by XRD, SEM and fluores⁃cence spectrophotometer. It was shown that the maximum of Ni doped content (x) was 0.03 and secondary phase NiO was observed while the Ni doped content (x) exceeded it. In pace with Ni doped content, red shift of ultravio⁃let absorption limit of Zn1-xNixO was observed and its energy band width was reduced gradually. The absorption of Zn1-xNixO in ultraviolet region was decreased but its absorption in visible region was enhanced. The strength of peak in emission spectroscopy of Zn1-xNixO was weakened and widened, and some new peak was observed.

关键词

氧化锌/镍掺杂/凝胶燃烧法/光致发光

Key words

ZnO/Ni doping/gel combustion method/photoluminescence

分类

通用工业技术

引用本文复制引用

陈建华,程好,赵俊锋..凝胶燃烧法制备镍掺杂氧化锌及其光致发光性能[J].Journal of Changshu Institute of Technology,2012,(4):6-9,4.

基金项目

新型功能材料重点实验室开放基金项目“染化敏化太阳能电池光阳极的制备及其性能的研究”(Kyz201017Z) (Kyz201017Z)

常熟理工学院青年教师科研启动项目“掺杂 ZnO 薄膜光阳极的制备及性能研究”(Kyz2010130Z) (Kyz2010130Z)

Journal of Changshu Institute of Technology

1008-2794

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