林产化学与工业2013,Vol.33Issue(4):43-47,5.DOI:10.3969/j.issn.0253-2417.2013.04.008
磷酸活化稻秆制备中孔活性炭的研究
Preparation of Mesoporous Activated Carbon from Rice Straw Using Phosphoric Acid
摘要
Abstract
Mesoperous activated carbon was prepared from rice straw by chemical activation with phosphoric acid and characterized by N2 adsorption,elemental analysis and scanning electron micrograph.The results showed that activated carbon was pre-ac-tivated at 140 ℃ for about 60 min and then prepared at the impregnated ratio 3:1 (mass ratio),activation temperature 450 ℃,activation duration 60 min.Under this condition,characteristics of activated carbon are:the yeild 25%,methylene blue adsorption value 215 mg/g,iodine adsorption values 835 mg/g,decolorization of caramel (A) 110%,ash content 3.03%,pecific surface area 967.7 m2/g,total volume 1.12 cm3/g,average pore diameter 4.6 rim.The ration of mesopores of activated carbon made from rice straw is 84.8 %.Rice straw can be used as the material to prepare activated carbon with mesoperes.关键词
稻秆/中孔活性炭/制备/化学法/表征Key words
rice straw/ mesoperous activated carbon/ preparation/ chemical activation/ characterization分类
化学化工引用本文复制引用
卢辛成,蒋剑春,孙康,谢新苹,王金表..磷酸活化稻秆制备中孔活性炭的研究[J].林产化学与工业,2013,33(4):43-47,5.基金项目
中国林科院林业新技术所基本科研业务费专项资金(CAFINT2013C02) (CAFINT2013C02)
江苏省自然科学基金(BK2012514) (BK2012514)