中国药房2013，Vol.24Issue(27)：2551-2553,3.DOI:10.6039/j.issn.1001-0408.2013.27.20
芪七连胶囊的质量标准研究
Study on Quality Standard of Qiqilian Capsule
摘要
Abstract
OBJECTIVE:To establish the quality standard for Qiqilian capsule.METHODS:TLC was used to identify Astragali Radix and Panax notoginseng.A HPLC-ELSD was used to measure the content of astragaloside Ⅳ in Qiqilian capsule.RESULTS:The qualitative identifications with TLC were specific without interference from negative control.The liner range of astragaloside Ⅳ were 0.529 5-4.2360 μg(r=0.9997) with average recovery of 99.34％ (RSD=1.10％,n=6).RSDs of precision,stability and reproducibility tests were all lower than 2％.CONCLUSIONS:Established standard can be adopted for the quality control of Qiqilian capsule.关键词
芪七连胶囊/质量标准/薄层色谱法/高效液相色谱-蒸发光散射检测器法/黄芪甲苷/黄芪/三七Key words
Qiqilian capsule/Quality standard/TLC/HPLC-ELSD/Astragaloside Ⅳ/Astragali Radix/Panax notoginseng分类
医药卫生引用本文复制引用
陈壮,岳桂华,黄敏,黄小鸥..芪七连胶囊的质量标准研究[J].中国药房,2013,24(27):2551-2553,3.基金项目
广西壮族自治区中医药管理局中医药科技专项资助课题(No.GZYZ1109) （No.GZYZ1109）
广西科学研究与技术开发计划项目(No.桂科攻0993003A-15) （No.桂科攻0993003A-15）
