现代农业科技Issue(18)：357-358,360,3.
固相萃取要高效液相色谱要荧光法测定食用菌中多菌灵的含量
Determination of Carbendazim in Edible Fungus by SPE-HPLC-FLD
张松成 1王小玲 1金锦长 1夏乐舜1
作者信息
- 1. 丽水出入境检验检疫局，浙江丽水 323000
- 折叠
摘要
Abstract
A new method was established for the determination of carbendazim in edible fungus by solid phase extraction-high performance liquid chromatography with fluorescence detector(SPE-HPLC-FLD). The edible fungus samples were extracted by ethyl acetate and purified by a solid phase extraction column. Then,the chromatographic separation was achieved on a C18 column. The mobile phase was 20 mmoL/L phosphate-acetonitrile. The results showed that the recovery rates of carbendazim were between 85.5%to 95.4%with the relative standard deviations below 6.0%,and limit of quantification(LOQs)was 0.05 mg/kg. The method is simple,sensitive,accurate,and repeatable,and can be used for determination of carben-dazim in edible fungus.关键词
食用菌/多菌灵/固相萃取/高效液相色谱/荧光检测/含量Key words
edible fungus/carbendazim/solid phase extraction/high performance liquid chromatography/fluorescence detection/content分类
化学化工引用本文复制引用
张松成,王小玲,金锦长,夏乐舜..固相萃取要高效液相色谱要荧光法测定食用菌中多菌灵的含量[J].现代农业科技,2013,(18):357-358,360,3.
