按摩与康复医学Issue(10):133-134,2.
HPLC法测定乳乐康凝胶膏剂中丁香酚的含量
The Determination for Content of Eugenol in Rulekang Gel Paste by HPLC
李智勇 1王洛临 1罗文汇 1杜建平 1陈朋1
作者信息
摘要
Abstract
Objective:To establish the determination for content of eugenol in Rulekang gel paste. Methods:Used high performance liquid chromatog-raphy (HPLC) to test the content of eugenol, chromatographic column:Kromasil C18 (4.6mm´250mm, 5µm) column;mobile phase:methanol-water (55:45);detection wavelength:280nm;flow rate:1.0ml/min;column temperature:30℃. Results:The eugenol had showed a good linear relationship in the range of 18.48~147.84µg/ml, r=0.99994, the average recovery was 98.18%, RSD was 1.06%(n=9). Conclusion:The method is accurate, reli-able and reproducible, and provides reference for quality controlling of Relekang gel paste.关键词
乳乐康凝胶膏剂/高效液相色谱法/丁香酚/含量测定Key words
Relekang gel patse/high performance liquid chromatography/eugenol/content determination分类
医药卫生引用本文复制引用
李智勇,王洛临,罗文汇,杜建平,陈朋..HPLC法测定乳乐康凝胶膏剂中丁香酚的含量[J].按摩与康复医学,2013,(10):133-134,2.