长沙理工大学学报（自然科学版）Issue(1)：93-98,6.
从晶体生长角度优化高性能磷酸银粉体的合成工艺
Technological parameter optimization for high performance Ag3 PO4 powders based on crystal growth mechanism
摘要
Abstract
A simple hydrothermal route is used to treat the Ag3 PO4 powders obtained by fast precipitation.Two key factors affecting the photocatalytic performance,crystallization qual-ity and specific surface area,are discussed based on crystal growth mechanism.Based on the XRD analysis,the crystallization factorξis introduced to evaluate the two factors,and the technological parameters are optimized for the synthesis of high performance Ag3 PO4 pow-ders.The results show,ξvalue is in good agreement with the photocatalytic performance of Ag3 PO4 powders,and it is very effective for technological parameter optimization.When the powders are treated under 148 ℃ for 12 h,ξvalue is the highest and the powders show excellent photocatalytic performance.关键词
Ag3PO4/水热法/X射线衍射/晶体生长/性能Key words
Ag3 PO4/hydrothermal/X-ray diffraction(XRD)/crystal growth/performance分类
化学化工引用本文复制引用
宋沿德,李雄波,刘国旺,陈春红,李培华,蔡富轩,陈曙光,李海斌..从晶体生长角度优化高性能磷酸银粉体的合成工艺[J].长沙理工大学学报（自然科学版）,2014,(1):93-98,6.基金项目
国家自然科学基金资助项目(51102025) （51102025）
湖南省自然科学基金资助项目(12JJ3039,14JJ7040) （12JJ3039,14JJ7040）
长沙市科技局科技计划项目(K1303005-11) （K1303005-11）
大学生研究性学习和创新性实验计划项目 （）
