哈尔滨商业大学学报（自然科学版）Issue(2)：224-228,5.
溶胶凝胶法制备二氧化锡纳米晶体
Preparation of tin dioxide nanocrystal by sol-gel methods
摘要
Abstract
With SnCl 4 · 5 H2 O as the precursor material , nanometer tin dioxide crystals were prepared using the sol -gel method .The tin dioxide crystals were characterized by X -ray diffraction (XRD) and scanning electron microscopy (SEM) analysis method.Furthermore, a series of investigations were performed about the influences of the ratio of reactants , the concentration of stannic chloride and the calcination temperature on the crystal structure of tin oxide nanoparticles , particles and dispersion .Results showed that on such conditions as the concentration of stannic chloride aqueous solution at 0.635 1 mol/L, ammonia solution at 4 mol/L, sintering powder for 3 h at 600℃, a good crystallization , a big specific surface ar-ea, and a good dispersion could be received .关键词
二氧化锡/纳米晶体/溶胶凝胶Key words
tin dioxide/nanocrystal/sol-gel分类
通用工业技术引用本文复制引用
王迪,田均庆,张书涛,张易楠,石海英,郑威..溶胶凝胶法制备二氧化锡纳米晶体[J].哈尔滨商业大学学报（自然科学版）,2014,(2):224-228,5.基金项目
教育部留学归国科研启动基金（20110039）；黑龙江省普通高等学校新世纪优秀人才培养计划（2010-15）；哈尔滨理工大学2013大学生创新实验项目． （）
