印染助剂Issue(12):45-47,3.
含氢硅油活泼氢含量的测定
Measurement of the active hydrogen content of hydrosilicone oil
方芳 1高慧莲 1张海婴1
作者信息
- 1. 浙江传化股份有限公司,浙江杭州 311215
- 折叠
摘要
Abstract
The measurement method of active hydrogen content of hydrosilicone oil was established through the reaction of hydrosilicone oil with bromine under acidic condition to generate hydrogen bromide, and the excess bromine reacted with potassium iodide, then the salting out iodine was measured with stan-dard titration of sodium thiosulfate solution. The effects of solvent types, the weight of sample, the amount of bromoacetic acid solution and potassium iodide and the reaction time on the measurement result were investi-gated.关键词
含氢硅油/活泼氢/溴-乙酸溶液/碘化钾Key words
hydrosilicone oil/active hydrogen/bromoacetic acid/potassium iodide分类
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方芳,高慧莲,张海婴..含氢硅油活泼氢含量的测定[J].印染助剂,2013,(12):45-47,3.