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含氢硅油活泼氢含量的测定

方芳 高慧莲 张海婴

印染助剂Issue(12):45-47,3.
印染助剂Issue(12):45-47,3.

含氢硅油活泼氢含量的测定

Measurement of the active hydrogen content of hydrosilicone oil

方芳 1高慧莲 1张海婴1

作者信息

  • 1. 浙江传化股份有限公司,浙江杭州 311215
  • 折叠

摘要

Abstract

The measurement method of active hydrogen content of hydrosilicone oil was established through the reaction of hydrosilicone oil with bromine under acidic condition to generate hydrogen bromide, and the excess bromine reacted with potassium iodide, then the salting out iodine was measured with stan-dard titration of sodium thiosulfate solution. The effects of solvent types, the weight of sample, the amount of bromoacetic acid solution and potassium iodide and the reaction time on the measurement result were investi-gated.

关键词

含氢硅油/活泼氢/溴-乙酸溶液/碘化钾

Key words

hydrosilicone oil/active hydrogen/bromoacetic acid/potassium iodide

分类

化学化工

引用本文复制引用

方芳,高慧莲,张海婴..含氢硅油活泼氢含量的测定[J].印染助剂,2013,(12):45-47,3.

印染助剂

OA北大核心CSTPCD

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