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响应面优化苹果皮渣多酚超声提取工艺研究

李珍 哈益明 李安 李伟明 王锋 李庆鹏

中国农业科学Issue(21):4569-4577,9.
中国农业科学Issue(21):4569-4577,9.DOI:10.3864/j.issn.0578-1752.2013.21.020

响应面优化苹果皮渣多酚超声提取工艺研究

Optimization of Ultrasound-Assisted Extraction Technology of Polyphenols from Apple Pomace by Response Surface Methodology

李珍 1哈益明 1李安 1李伟明 1王锋 1李庆鹏1

作者信息

  • 1. 中国农业科学院农产品加工研究所/农业部农产品加工与质量控制重点实验室,北京 100193
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摘要

Abstract

[Objective]The objective of this study is to optimize ultrasound-assisted ethanol extraction of polyphenols from apple pomace. [Method]Residues from juice extraction of apple were used in this paper. On the basis of single-factor test, the response surface methodology was used to investigate the effects of processing parameters, including extraction time, temperature, ultrasound power and solvent/material ratio. The extraction rate of polyphenols was chosen as response value, mathematical model was established by implementing four factors and three levels. [Result] The model was of great difference, and the established regression equation for polyphenols yield had an excellent goodness of fit. Therefore the polyphenols from apple pomance could be analyzed and predicted by the model. Factors influencing the extraction of polyphenols from the apple pomace were in the order as follows:extraction temperature>solvent/material ratio>ultrasound power>extraction time. The response surface plots showed that the interaction between extraction time and ultrasound power was not significant, while the interaction between extraction temperature and ultrasound power was outstanding, and the main effect of solvent/material ratio was greater than the temperature. The optimum technological conditions were extraction time of 10 min, extraction temperature of 65℃, ultrasonic p solvent/material ratio of 1﹕30(g·mL-1).[Conclusion]The extraction ratio of apple polyphenols was up to 4.53 mg·g-1, which is highly consistent with the predictive value of 4.55 mg·g-1.

关键词

苹果皮渣/多酚/超声波/响应面

Key words

apple pomace/polyphenols/ultrasound assisted/response surface methodology

引用本文复制引用

李珍,哈益明,李安,李伟明,王锋,李庆鹏..响应面优化苹果皮渣多酚超声提取工艺研究[J].中国农业科学,2013,(21):4569-4577,9.

基金项目

农业部公益性行业科研专项(201303076)、中国农业科学院基本科研业务费预算增量项目(2013ZL015)、国家“863”计划子课题 ()

中国农业科学

OA北大核心CSCDCSTPCD

0578-1752

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