中国烟草学报Issue(6)：25-33,9.DOI:10.3969/j.issn.1004-5708.2013.06.004
离子色谱法同时测定烟草中的硝酸盐与亚硝酸盐
Simultaneous determination of nitrate and nitrite in tobacco by ion exchange chromatography
摘要
Abstract
A sensitive ion exchange chromatography method was developed for simultaneous determination of nitrate and nitrite in tobacco. Ultrapure water was used for ultrasound-assisted solvent condition. Extract liquor were separated using anion exchange column. Nitrate and nitrite ion were then detected by conductance detector. Results showed that linear relations were observed in the range of 0.032~1.600 mg/L for nitrite,and 0.800~40.000 mg/L for nitrate. Detection limits were 1.06 mg/kg for nitrate and 1.23 mg/kg for nitrite. Recoveries were 96.3%~99.0% for nitrate and 96.1%~101.6% for nitrite. Both RSDs were below 5%.关键词
烟草/硝酸盐/亚硝酸盐/离子色谱法Key words
tobacco/nitrate/nitrite/ion exchange chromatography分类
轻工纺织引用本文复制引用
张建平,黄朝章,邓其馨,苏明亮,谢卫,许寒春,刘泽春,吴清辉..离子色谱法同时测定烟草中的硝酸盐与亚硝酸盐[J].中国烟草学报,2013,(6):25-33,9.基金项目
国家烟草专卖局卷烟减害技术重大专项子项目“‘七匹狼’卷烟主流烟气7种成分释放量影响因素研究” （）
