中国中医药信息杂志Issue(11)：47-48,49,3.DOI:10.3969/j.issn.1005-5304.2013.11.017
健脾复肝丸质量标准研究
Study on Quality Standard of Jianpi Fugan Pills
郑光明 1宋宏安1
作者信息
- 1. 荆门市中医医院，湖北 荆门 448000
- 折叠
摘要
Abstract
Objective To establish the quality standard for Jianpi Fugan Pills. Methods Angelicae Sinenis Radix and Atractylodis Macrocephalae Rhizome in the formulation were qualitatively identified by TLC. The content of ferulic acid was analyzed by HPLC. TIANHE C18 column (250 mm×4.6 mm, 5 µm) was used with a mobile phase of acetonitrile-0.085% phosphorous acid (17∶83). The content was detected at wavelength of 323 nm. The flow rate was 1.0 mL/min, and temperature was 25 ℃. Results The spots in the TLC of Angelicae Sinenis Radix and Atractylodis Macrocephalae Rhizome were in the same chormatograms of control articles. The linear range of ferulic acid was 0.114-1.482 µg. The average recovery was 98.36%and RSD was 1.16%. Conclusion The method is simple, accurate and highly sensitive, which can be used for quality control of Jianpi Fugan Pills.关键词
健脾复肝丸/阿魏酸/薄层色谱法/高效液相色谱法Key words
Jianpi Fugan Pills/ferulic acid/TLC/HPLC分类
医药卫生引用本文复制引用
郑光明,宋宏安..健脾复肝丸质量标准研究[J].中国中医药信息杂志,2013,(11):47-48,49,3.
