重庆理工大学学报（自然科学版）Issue(12)：71-75,5.DOI:10.3969/j.issn.1674-8425(z).2014.12.014
肉桂酸环己酯催化合成工艺
Study on Technology of Catalytic Synthesis of Cyclohexyl Cinnamate
摘要
Abstract
Cyclohexyl cinnamate was catalytic synthesized by cinnamic acid and cyclohexanol. The tyPe of catalysts and dosage,the molar ratio of cinnamic acid and cyclohexanol,and the reaction time were exPlored by single factor exPeriment and orthogonal exPeriment. The results show that the oPti-mal conditions of cyclohexyl cinnamate is that when the sodium bisulfate is the catalyst,and its dosage is 0. 5g,and the molar ratio of cinnamic acid and cyclohexanol is 1:4,and the reaction time is 1h, the yield of cyclohexyl cinnamate is uP to 94. 6%. The method has advantages of simPle oPeration, mild reaction conditions,short reaction time,and high Product Purity.关键词
肉桂酸环己酯/肉桂酸/硫酸氢钠/催化合成Key words
cyclohexyl cinnamate/cinnamic acid/sodium bisulfate/catalytic synthesis分类
化学化工引用本文复制引用
黄飞,屈飞强,任晓琼..肉桂酸环己酯催化合成工艺[J].重庆理工大学学报（自然科学版）,2014,(12):71-75,5.基金项目
国家级大学生创新创业训练计划项目（201410375003）；安徽省大学生创新创业训练项目 （）
