吉林医药学院学报Issue(1):15-17,3.
液相微萃取HPLC测定消癌平口服液中绿原酸含量
The determination of chlorogenic acid content in Xiao'aiping oral liquid by liquid phase microextraction HPLC
张敏 1李海茹2
作者信息
- 1. 空军太原干休所卫生所,山西 太原 030006
- 2. 山西省肿瘤医院药学部,山西 太原030013
- 折叠
摘要
Abstract
Objective To study the quantitative method for chlorogenic acid in Xiao'aiping oral liquid .Methods High performance liquid chromatography ( HPLC) were employed.Chromatographic column was Eclipse XDB-C18 column (150 mm ×4.6 mm ×5μm),mobile phase was acetonitrile-0.4%phosphoric acid solution (8∶92);and de-tection wavelength was 327 nm.Results The linear range of chlorogenic acid covered from 1.60μg to 160μg (r=0.999 5,n=5),and the average sample recovery rate was 99.3%,RSD=2.4%.Conclusion This method is sim-ple,sensitive,accurate,and can be for Xiao'aiping oral liquid quality control .关键词
消癌平口服液/绿原酸/液相微萃取Key words
Xiao'aiping oral liquid/chlorogenic acid/the liquid phase microextraction分类
医药卫生引用本文复制引用
张敏,李海茹..液相微萃取HPLC测定消癌平口服液中绿原酸含量[J].吉林医药学院学报,2015,(1):15-17,3.