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分级结构氧化锌的制备及形貌调控

沈俊海 李佳佳 李良超 李涓碧 丁艳

高等学校化学学报Issue(6):1135-1141,7.
高等学校化学学报Issue(6):1135-1141,7.DOI:10.7503/cjcu20140083

分级结构氧化锌的制备及形貌调控

Fabrication and Morphological Control of Hierarchical-structure ZnO

沈俊海 1李佳佳 1李良超 1李涓碧 1丁艳1

作者信息

  • 1. 浙江师范大学化学系,先进催化材料教育部重点实验室,金华 321004
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摘要

Abstract

The hierarchical-structure ZnO with different morphologies were fabricated by the hydrothermal method respectively using single and mixed zinc salts as the zinc source, sodium hydroxide as the precipitant, alanine and ionic liquid(IL) as the surfactant. The samples were characterized by XRD analysis, SEM obser-vation, IR and UV-Vis spectrometry. The influential factors of the sample morphology were discussed, which included the zinc source(single, double and three zinc salts), the kind and dosage of ionic liquid, the dosage of alanine and temperature, etc. The modulation of anionic on sample morphology was speculated in the forma-tion process of the ZnO with hierarchical structure.

关键词

氧化锌/分级结构/水热法/形貌

Key words

ZnO/Hierarchical structure/Hydrothermal method/Morphology

分类

化学化工

引用本文复制引用

沈俊海,李佳佳,李良超,李涓碧,丁艳..分级结构氧化锌的制备及形貌调控[J].高等学校化学学报,2014,(6):1135-1141,7.

基金项目

国家自然科学基金(批准号:21071125)资助. Supported by the National Natural Science Foundation of China(No.21071125) (批准号:21071125)

高等学校化学学报

OA北大核心CSCDCSTPCD

0251-0790

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