高等学校化学学报Issue(7)：1523-1528,6.DOI:10.7503/cjcu20140065
Ag+/Ag/ZnO 多孔纳米结构纤维材料的制备及可见光催化性能
Preparation and Visible-light Catalytic Property of Ag+/Ag/ZnO Porous Nano-structured Fiber Materials
摘要
Abstract
Ag+ / Ag / ZnO porous nano-structured fiber materials were prepared by the template-assisted two-steps method and characterized by thermogravimetric analysis(TG), X-ray diffraction(XRD), X-ray photoe-lectron spectroscopy(XPS), scanning electron microscopy(SEM) and UV-Vis spectroscopy(UV-Vis) tech-niques. The effect of modified silver amount(molar fraction, 0-1. 5% ) on the photocatalytic property of ZnO materials was studied by the degradation of methylene blue(MB) as the model reaction. The results show that the Ag+-Ag co-modified ZnO porous nano-structured fiber materials are successfully prepared via the template-assisted two-steps method and the Ag+-Ag co-modifification affects the photocatalytic performance of ZnO mate-rials by affecting its cell structure and light adsorption property and morphology. Under the irradiation of visi-ble light, the Ag+ / Ag / ZnO porous nano-structured fiber materials showed better catalytic performance than pure ZnO and the catalytic perfrmace of Ag+ / Ag / ZnO is related to the modified amount of Ag+-Ag. In this pa-per, the way of Ag+ and Ag for improving photocatalytic performance of the ZnO materials was discussed. And the obtained results are helpful to understand the photocatalytic phenomena and mechanisms on the multi-structured material.关键词
Ag+ / Ag/ ZnO/多孔纳米结构纤维材料/模板辅助两步法/光催化性能Key words
Ag+/Ag/ZnO/Porous nano-structured fiber material/Template-assisted two-steps method/Photocatalytic property分类
化学化工引用本文复制引用
邵克让,李建娇,安兴才,雷自强,苏碧桃..Ag+/Ag/ZnO 多孔纳米结构纤维材料的制备及可见光催化性能[J].高等学校化学学报,2014,(7):1523-1528,6.基金项目
国家自然科学基金(批准号:21174114)、教育部“长江学者和创新团队发展计划”创新团队项目(批准号：IRT1177)、甘肃省科技计划项目(批准号:1204GKCA006)、甘肃省自然科学基金(批准号:1010RJZA024)和西北师范大学科技创新项目(批准号:nwnu-kjcxgc-03-63)资助. Supported by the National Natural Science Foundation of China(No.21174114), the Program for Changjiang Scholars and Innovative Re-search Team in University of Ministry of Education of China(No. IRT1177), the Scientific and Technical Plan Project of Gansu Province, China (No.1204GKCA006), the Natural Science Foundation of Gansu Province, China(No.1010RJZA024) and the Scientific and Technical Innovation Project of Northwest Normal University, China(No. nwnu-kjcxgc-03-63) （批准号:21174114）
