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钼酸铵分光光度法检测糖厂工业磷酸含量的应用研究

莫佳琳 张思原 陆海勤 陆芳启 马丽霞 覃胜尊 黄声威

甘蔗糖业Issue(1):52-56,5.
甘蔗糖业Issue(1):52-56,5.

钼酸铵分光光度法检测糖厂工业磷酸含量的应用研究

The Research of Phosphoric Acid Content Detection by Ammonium Molybdate Spectrophotometry

莫佳琳 1张思原 2陆海勤 2陆芳启 2马丽霞 2覃胜尊 2黄声威2

作者信息

  • 1. 广西壮族自治区产品质量监督检验研究院,广西南宁530007
  • 2. 广西大学轻工与食品工程学院,广西南宁530004
  • 折叠

摘要

Abstract

Based on ammonium molybdate spectrophotometric method, a detection method was established to determine industrial phosphoric acid content. Recovery of sample was between 100%~109%; the relative standard deviation of test results precision was less than 4.0%; the concentration of sample phosphorus had a preferable linear correlation in the range of 0.02~0.72 mg/L, method for synthesis uncertainty was about 1.8041%; specificity experiments showed that phosphoric acid with impurity did not affect the accuracy of measurement. The average to determine two industrial phosphoric acid with 85% concentration were 84.738% and 83.152%, and the average recovery were 100.20% and 104.09%. Ammonium molybdate spectrophotometric method can apply to the determination of phosphate content in sugar mill industry.

关键词

工业磷酸/钼酸铵/检测/验证

Key words

Industrial phosphoric acid/Ammonium molybdate/Detection/Validation

分类

轻工纺织

引用本文复制引用

莫佳琳,张思原,陆海勤,陆芳启,马丽霞,覃胜尊,黄声威..钼酸铵分光光度法检测糖厂工业磷酸含量的应用研究[J].甘蔗糖业,2015,(1):52-56,5.

基金项目

广西自然科学基金项目(2013GXNSFAA019049) (2013GXNSFAA019049)

甘蔗糖业

OACSTPCD

1005-9695

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