药学研究Issue(5)：272-273,2.
微波消解-石墨炉原子吸收分光光度法测定米格列醇中的钯
Determination of pd in miglitol by microWave digestion - graphite furnace atomic absorption spectrometry
邵俊平 1郝贵周 2吴善霞2
作者信息
- 1. 费县食品药品监督管理局，山东 临沂 273499
- 2. 鲁南制药集团有限公司，山东 临沂 276006
- 折叠
摘要
Abstract
Objective To establish a method for the determination of Pd in miglitol by graphite furnace atomic absorp-tion spectrometry. Methods Palladium hollow cathode lamp was used. The detection wavelength was 247. 6 nm. Graphite Furnace Atomizer was adopted. Results The linear range of Pd was 0. 0 ~ 140. 0 μg·L - 1(r = 0. 998 3),the average re-covery was 94. 4% and the RSD was 3. 5%(n = 6). Conclusion This method can be used to determine residual Pd in miglitol.关键词
微波消解/石墨炉原子吸收分光光度法/米格列醇/钯Key words
Microwave digestion/Graphite furnace atomic absorption spectrometry/Miglitol/Palladium分类
医药卫生引用本文复制引用
邵俊平,郝贵周,吴善霞..微波消解-石墨炉原子吸收分光光度法测定米格列醇中的钯[J].药学研究,2014,(5):272-273,2.
