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气相色谱法测定麝香保心丸中冰片和麝香酮的含量

张楠 艾芸

陕西中医Issue(7):903-904,2.
陕西中医Issue(7):903-904,2.DOI:10.3969/j.issn.1000-7369.2015.07.071

气相色谱法测定麝香保心丸中冰片和麝香酮的含量

Determinnation of borneol and muscone in Shexiang Baoxin Pills by GC

张楠 1艾芸1

作者信息

  • 1. 西安市食品药品检验所 西安710054
  • 折叠

摘要

Abstract

Objective:To establish the methods for determing borneol and Musk ketone in Shexiang Baoxin Pills .Method:GC(Thermo‐TG‐WAXMS capillary column ;FID as detector)were used ,The column temperature was rose by program .Results :A good linearity relationship with the peak areas was exhibited when the sample size of borneol and Musk ketone were in the range of 32 .06~513 .02μg/mL (r=0 .9997) and y=8 .1037x -0 .7348μg/mL(r=0 .9995) re‐spectively ,The average rate of recovery was 98 .7% and 98 .6% .Conclusion:The method is simple、accurate、and highly sensitive and suitable for Shexiang Baoxin Pills .

关键词

色谱法,气相/麝香保心丸/麝香酮/冰片

Key words

Gaschromatography/Shexiang Baoxin Pills/Borneol/Muskketone

分类

医药卫生

引用本文复制引用

张楠,艾芸..气相色谱法测定麝香保心丸中冰片和麝香酮的含量[J].陕西中医,2015,(7):903-904,2.

陕西中医

OACSTPCD

1000-7369

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