世界中医药Issue(10)：1355-1357,3.DOI:10.3969/j.issn.1673-7202.2014.10.030
川贝止咳合剂质量标准研究
Study on Quality Standard of Chuanbeizhike Mixture
孙冬梅 1汪梦霞 2董玉娟2
作者信息
- 1. 广东省中医药工程技术研究院，广州，510095
- 2. 广州中医药大学，广州，510405
- 折叠
摘要
Abstract
Objective:To establish the quality standard of Chuanbeizhike mixture.Methods:Thin layer chromatography ( TLC) was used to identify Fructus Aurantii, Radix Platycodonis in Chuanbeizhike Mixture.Naringin in Fructus Aurantii was determined by high per-formance liquid chromatography ( HPLC) .Results:The TLC spots of Fructus Aurantii and Radix Platycodonis were clear with good reso-lution and free of interference of negative samples.The calibration curve of HPLC was linear in the range of 160~800ng (r=0.999 9). The average recovery rate was 98.90%, RSD=1.32%.Conclusion:The method is rapid, curate, sensitive and reliable, and it can be used to control the quality of Chuanbeizhike Mixture.关键词
川贝止咳合剂/薄层色谱法/高效液相色谱法/质量标准/柚皮苷Key words
Chuanbeizhike Mixture/TLC/HPLC/Quality standard/Naringin分类
医药卫生引用本文复制引用
孙冬梅,汪梦霞,董玉娟..川贝止咳合剂质量标准研究[J].世界中医药,2014,(10):1355-1357,3.
