世界中医药Issue(3)：420-422,3.DOI:10.3969/j.issn.1673-7202.2015.03.030
GC 法测定羚黄宝儿丸中麝香酮、冰片、丁香酚的含量
Determination of Contents of Muscon,Borneol and Eugenol in Linghuangbaoer Pellets by GC Method
任睿 1陈新国 1李磊 2袁少雄 2陈娇娇 2张园园2
作者信息
- 1. 广东省药品检验所，广州，510000
- 2. 北京中医药大学中药学院，北京，100102
- 折叠
摘要
Abstract
Objective:To determine the contents of Muscon,Borneo and Eugenol in Linghuangbaoer Pellets by GC method.Meth-ods:The GC system consisted of DB-WAX(30.0 m ×0.25 mm ×0.25 μm)capillary column.Programmed temperature was set from 120 ℃ to 210 ℃ and the detector temperature was 250 ℃.The detector was FID using high pure helium as carrier gas with the flow rate of 1.2 mL/min.Results:Borneol,Eugenol and Muscon were separated with a good linearity in the sample size ranges of 0.125 ~2 mg/mL for Borneol,0.05 ~0.8 mg/mL for Eugenol,and 0.005 ~0.08 mg/mL for Muscon.The average recoveries for Borneol,Eugenol and Muscon was 105.51% (RSD =1.44%),95.79% (RSD =0.29%),99.94% (RSD =0.66%),respec-tively.Conclusion:The GC method is simple,feasible and reproducible.It can be used for the quality control of Linghuangbaoer Pellets.关键词
羚黄宝儿丸/麝香酮/冰片/丁香酚/含量Key words
GC/Linghuangbaoer Pellets/Muscon/Borneol/Eugenol分类
医药卫生引用本文复制引用
任睿,陈新国,李磊,袁少雄,陈娇娇,张园园..GC 法测定羚黄宝儿丸中麝香酮、冰片、丁香酚的含量[J].世界中医药,2015,(3):420-422,3.
