特产研究Issue(4):22-27,6.
人参皂苷在正丁醇/水二相分配关系的研究
Distribution Relationship of Ginsenosidesin N -butanol Phase and Water Phase
摘要
Abstract
Ginsenosides distribution rules in n -butanol phase and water phase were studied ,to provide the basis for separation and analysis of ginsenosides .After solution of ginseng root was extracted with n -butanol saturated water ,ginsenoside content Rb1 ,Rb2 ,Rc ,Rd ,Rg1 ,Re ,Rf , Ro in two phases were detected with HPLC/MS ,as well as 9 kinds of malonyl-ginsenosides .Results:Distribution ratio of different ginsenosides in the biphase vary greatly ,malonyl-ginsenosides distribution ratio in water phase was larger than that in n -butanol phase while neutral gin-senosides appears a different side .Conclusion:After extracted three times with n -butanol saturated water ,substantially all of the neutral gin-senosides were transferred to n -butanol phase;the ratio of malonyl -ginsenosides in n-butanol phase to water phase is 3∶2 .关键词
人参/人参皂苷/丙二酰基人参皂苷/水/油分配Key words
Ginseng/ginsenosides/maonyl-ginsenosides/water/oil distribution分类
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王玉帅,金银萍,郑培和,刘俊霞,肖盛元,王英平,袁忠久..人参皂苷在正丁醇/水二相分配关系的研究[J].特产研究,2014,(4):22-27,6.基金项目
吉林省发展规划项目(201302040509YY );北京市自然基金 ()