西北师范大学学报(自然科学版)Issue(2):47-51,5.
纳米 TiO2颗粒的水解制备及其光催化性能研究
Hydrolysis preparation of TiO 2 nanomaterials and its photocatalytic performance
摘要
Abstract
Different TiO2 nanostructures are prepared by hydrolyzed the tetrabutyl titanate in HCl , CH3 COOH , NH3 ・ H2 O and NaOH solutions , respectively , and then annealed at 500 ℃ in air . The structure of samples are tested by scanning electron microscopy ( SEM ) , high‐resolution transmission electron microscopy(HR‐TEM ) ,X‐ray diffraction pattern (XRD)and Raman spectra . Their phohocatalytic performance are tested by photo‐degradation of Rhodamine B ( RhB ) dye . The concentration of Rhodamine B molecule is measured by UV spectrophotometer . The results show that the obtained sample are anatase TiO 2 nanostructures . The morphology of the samples are different for different hydrolysis solution .Because of its excellent surface sturcture , the TiO2 nanomaterial prepared in CH3 COOH solution has good photocatalytic performance .关键词
TiO2/水解/钛酸四丁酯/光催化Key words
titania oxide/hydrolysis/tetrabutyl titanate/photocatalysis分类
化学化工引用本文复制引用
张海军,滕凤,张振兴,谢二庆..纳米 TiO2颗粒的水解制备及其光催化性能研究[J].西北师范大学学报(自然科学版),2015,(2):47-51,5.基金项目
国家自然科学基金资助项目(U1232121);甘肃省自然科学基金资助项目 ()