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高效液相色谱法测定纺织品中三氯生的研究

潘建君 张晓婷 陆勋元 闵洁

印染助剂Issue(10):50-52,3.
印染助剂Issue(10):50-52,3.

高效液相色谱法测定纺织品中三氯生的研究

Study on the determination of triclosan in textiles by high performance liquid chromatography (HPLC)

潘建君 1张晓婷 1陆勋元 1闵洁2

作者信息

  • 1. 湖州出入境检验检疫局,浙江湖州 313000
  • 2. 东华大学生态纺织教育部重点实验室,上海 201620
  • 折叠

摘要

Abstract

The optimal method of measuring triclosan in textiles by high performance liquid chromatogra-phy was determined through investigation of parameters of high performance liquid chromatography, condi-tions of extraction, lowest limit, recover ratio and repeatability. Triclosan in textiles was extracted by 25 mL methyl alcohol for 30 min, then detected by HPLC (wave-length was 282 nm). The linear correlation coeffi-cient was 0.999 8 in the range of 0.1~100 mg/L. The detection limit was 1 mg/kg, and the recoveries were in the range of 86%~103%.

关键词

纺织品/三氯生/高效液相色谱

Key words

textiles/triclosan/high performance liquid chromatography

分类

轻工纺织

引用本文复制引用

潘建君,张晓婷,陆勋元,闵洁..高效液相色谱法测定纺织品中三氯生的研究[J].印染助剂,2014,(10):50-52,3.

基金项目

浙江出入境检验检疫局科技计划项目 ()

印染助剂

OA北大核心CSTPCD

1004-0439

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