印染助剂Issue(10):50-52,3.
高效液相色谱法测定纺织品中三氯生的研究
Study on the determination of triclosan in textiles by high performance liquid chromatography (HPLC)
摘要
Abstract
The optimal method of measuring triclosan in textiles by high performance liquid chromatogra-phy was determined through investigation of parameters of high performance liquid chromatography, condi-tions of extraction, lowest limit, recover ratio and repeatability. Triclosan in textiles was extracted by 25 mL methyl alcohol for 30 min, then detected by HPLC (wave-length was 282 nm). The linear correlation coeffi-cient was 0.999 8 in the range of 0.1~100 mg/L. The detection limit was 1 mg/kg, and the recoveries were in the range of 86%~103%.关键词
纺织品/三氯生/高效液相色谱Key words
textiles/triclosan/high performance liquid chromatography分类
轻工纺织引用本文复制引用
潘建君,张晓婷,陆勋元,闵洁..高效液相色谱法测定纺织品中三氯生的研究[J].印染助剂,2014,(10):50-52,3.基金项目
浙江出入境检验检疫局科技计划项目 ()