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反相高效液相色谱法测定洗涤用品中的烷基酚聚氧乙烯醚

李晓睿 姚晨之 严方

印染助剂Issue(6):50-52,3.
印染助剂Issue(6):50-52,3.

反相高效液相色谱法测定洗涤用品中的烷基酚聚氧乙烯醚

Determination of alkylphenol polyoxyethylene ether in detergents by RP-HPLC method

李晓睿 1姚晨之 1严方1

作者信息

  • 1. 中国日用化学工业研究院,山西太原 030001
  • 折叠

摘要

Abstract

A method of liquid chromatography-diode array detector was set up to detect octylphenol, non⁃ylphenol, polyoxyethylene octylphenol ether and polyoxyethylene nonylphenol ether in detergents. The results showed that at the selected conditions, the detergent of these four substances could be wel separated from other surfactants. Within the concentration range of 0.02~0.50 g/L, these four compounds had good linear rela⁃tionship between peak area and concentration, the determination limit was 0.48~0.67 μg/L, the relative stan⁃dard deviation (RSD) ranges were 0.08%~1.79%, and the recovery of the samples were 96.7%~104.2%. This method is simple, quick and has good reproducibility, which is suitable for detection of alkylphenol polyoxyeth⁃ylene ether in the household detergent products.

关键词

液相色谱/烷基酚聚氧乙烯醚/洗涤剂/检测

Key words

liquid chromatography/alkylphenol polyoxyethylene ether/detergent/detection

分类

化学化工

引用本文复制引用

李晓睿,姚晨之,严方..反相高效液相色谱法测定洗涤用品中的烷基酚聚氧乙烯醚[J].印染助剂,2015,(6):50-52,3.

印染助剂

OA北大核心CSTPCD

1004-0439

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