中国药物评价Issue(2)：83-86,4.
大七厘散的质量标准研究
Study of the Quality Standards of Daqili Powder
摘要
Abstract
Objective:To establish quality control for Daqili Powder.Methods: Rhei Radix et Rhizoma, Angelicae sinensis Radix, Borneolum Syntheticum,Notoginseng Radix et Rhizoma, Drynariae Rhizoma in Daqili Powder were identified by TLC,and draorhodin was determined by HPLC.Test solution was made with 12%phosphoric acid in methanol,Use a mixture of acetonitrile and 0.05 mol· L-1 so-dium dihydrogen phosphate solution (50∶50) as the mobile phase.As detector a spectrophotometer set at 440 nm.Results:The calibration curves were linear within the range of 0.774~77.415 μg· mL-1 ( r=0.9999 ).The average recovery was 100.2% with RSD was 1.8%( n=9).Conclusion:The method is sensitive and accurate,and it is suitable for the quality control of Daqili Powder.关键词
大七厘散/血竭素/大黄/当归/冰片/三七/骨碎补/质量标准Key words
Daqili Powder/Dracorhodin/Rhei Radix et Rhizoma/Angelicae sinensis Radix/Borneolum Syntheticum/Notoginseng Radix et Rhizoma/Drynariae Rhizoma/Quality control分类
医药卫生引用本文复制引用
陈惠玲,胡珊梅,陈洁,李玲玲,黄惠琼..大七厘散的质量标准研究[J].中国药物评价,2015,(2):83-86,4.基金项目
2012年厦门市重大科技项目，项目编号3502Z20121035 （）
