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保妇康泡沫剂的质量控制

张志勇 鲍家科 茅向军

中国药业Issue(13):22-23,24,3.
中国药业Issue(13):22-23,24,3.

保妇康泡沫剂的质量控制

Quality Control of Baohukang Foaming Agent

张志勇 1鲍家科 1茅向军1

作者信息

  • 1. 贵州省食品药品检验所,贵州 贵阳 550004
  • 折叠

摘要

Abstract

Objective To establish the quality standard for Baohukang Foaming Agent ( zedoary turmeric oil, borneol ) . Methods Zedoary turmeric oil and borneol in the preparation were identified by Thin layer chromatography ( TLC ) . The content of borneol was determined by gas chromatography ( GC ) with using the Elite Wax column ( 30 m × 0. 32 mm,0. 25μm ) and adopting the FID detector with the col-umn temperature programming. Results The TLC was distinct with good separation and without the negative interference;the linearity of borneol in the sample size was in the range of 0. 292 0-2. 952 0 mg/mL ( r=0. 999 2 ) . The average recovery rate for borneol was 98. 39%, RSD was 1. 18% ( n=9 ) . Conclusion This method is convenient and easy to operate, accurate and reliable in the detection results, which can be applied to control the quality of Baohukang Foaming Agent.

关键词

保妇康泡沫剂/定性鉴别/气相色谱法/冰片

Key words

Baohukang Foaming Agent/Thin layer chromatography/gas chromatography/borneol

分类

医药卫生

引用本文复制引用

张志勇,鲍家科,茅向军..保妇康泡沫剂的质量控制[J].中国药业,2014,(13):22-23,24,3.

基金项目

国家药品标准提高研究项目,项目编号ZN-049。 ()

中国药业

1006-4931

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