中国药业Issue(17):28-29,2.
微波消解-石墨炉原子吸收分光光度法测定可吸收性外科缝线中重金属铬含量
Determination of Heavy Metal Chromium Content in Absorbable Surgical Suture by Microwave Digestion-Graphite Furnace Atomic Absorption Spectrophotometry
张成 1王刚林 2黎隽 1王辉1
作者信息
- 1. 陕西省医疗器械检测中心,陕西 西安 710075
- 2. 重庆医疗器械质量检验中心,重庆 401147
- 折叠
摘要
Abstract
Objective To establish a determination method of heavy metal chromium ( Cr ) content in the absorbable surgical suture. Methods The microwave digestion-graphite furnace atomic absorption spectrophotometry was used to determine the Cr content in the absorbable surgical suture. Results The calibration curve of Cr showed good linearity in the range of 0-10μg/L, Y=0. 051 05 X-0. 038 3, r=0. 997 6 ( n=5 ) , the average recovery rate of Cr was 95. 74%, RSD was 0. 63%( n=6 ) . Conclusion This method is rapid, simple, ac-curate and reliable with good reproducibility, which can be used to determine heavy metal Cr content in the absorbable surgical suture.关键词
可吸收性外科缝线/原子吸收石墨炉法/重金属/铬Key words
absorbable surgical suture/graphite furnace atomizer/heavy metal chromium/Cr分类
医药卫生引用本文复制引用
张成,王刚林,黎隽,王辉..微波消解-石墨炉原子吸收分光光度法测定可吸收性外科缝线中重金属铬含量[J].中国药业,2014,(17):28-29,2.