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反相高效液相色谱法测定血安胶囊中没食子酸含量

黄花红

中国药业Issue(7):51-52,2.
中国药业Issue(7):51-52,2.

反相高效液相色谱法测定血安胶囊中没食子酸含量

Determination of Gallic Acid Content in Xuean Capsule by RT - HPLC

黄花红1

作者信息

  • 1. 江苏省淮安市妇幼保健院,江苏 淮安 223001
  • 折叠

摘要

Abstract

Objective To establish a RT - HPLC method for determining the gallic acid content in Xuean Capsule by RP - HPLC. Methods The octadecyl silane bonded silica gel column ODS - C18 was adopted with the mixture solvent of methanol - 0. 1% phospho-ric acid (3 : 97) as the mobile phase, the flow rate was 1. 0 mL / min and the detecting wavelength was 214 nm. Results The sample size of gallic acid in the range of 0. 021 1 - 0. 211 μg / mL showed the good linear relation with the peak area. The average recovery rate was 99. 28% , RSD = 1. 73% ( n = 6 ) . Conclusion It is concluded that with the parameter set used in this study, the gallic acid content in Xuean capsules can be determined in a fast and accurate manner with a good reproducibility.

关键词

血安胶囊/没食子酸/高效液相色谱法

Key words

Xuean capsules/gallic acid/HPLC

分类

医药卫生

引用本文复制引用

黄花红..反相高效液相色谱法测定血安胶囊中没食子酸含量[J].中国药业,2015,(7):51-52,2.

中国药业

1006-4931

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