中国药业Issue(13):28-29,2.
参芎葡萄糖注射液中总酚酸含量测定方法研究
Study on Measurement Method of Total Phenolic Acid Content in Shenxiong Glucose Injection
摘要
Abstract
Objective To establish a method for the determination of total phenolic acid in Shenxiong Glucose Injection. Methods The UV spectrophotometry was adopted with protocatechuic aldehyde as the reference substance, the total phenolic content in Shenxiong Glu-cose Injection was measured. Results The mass concentration of total phenolic acids in the range of 0. 008-0. 030 g/L demonstrated the good linear relation with the absorbance, A=31. 541 04 C-0. 103 97, r=0. 999 6 ( n=5 ) , the average recovery rate was 103. 61% , RSD=4. 85% ( n=9 ) . Conclusion The method is simple, accurate and reliable, and can be used as the quality control method of Shenxiong Glucose Injection.关键词
参芎葡萄糖/总酚酸/含量测定/紫外分光光度法Key words
Shenxiong Glucose Injection/total phenolic acid/content determination/ultraviolet spectrophotometry分类
医药卫生引用本文复制引用
朱迪,谭丹,侯靖宇,王爱民,兰燕宇,郑林..参芎葡萄糖注射液中总酚酸含量测定方法研究[J].中国药业,2015,(13):28-29,2.基金项目
国家科技支撑计划课题,项目编号2013BAI11B01;贵州省科技重大专项,项目编号黔科合重大专项字[2011]6019号;贵州省中药现代化专项,项目编号黔科合中药字[2013]5062号。 ()