中医药学报Issue(6)：11-13,3.
五味子糖浆中五味子木脂素类成分的含量测定
Determination of Mixed ZiMu Lipid Classes in Wuweizi Syrup
摘要
Abstract
Objective:To establish the determination method of Schizandrin, Aomisin and Deoxyschizandrin in Wuweizi syrup with RP-HPLC.Methods:The samples were analyzed on a XDB C18 column (5μm,4.6mm ×250mm) by using formaldehyde-water as the mobile phase at the flow rate of 1.0mL/min,250nm as the detection wave-length.Re-sults:Schizandrin showed a good relationship at the range of 0.04 ~2.02mg/ml (r=1).Regression Equation:y=10311x-23.19.The average recovery of syringin was 98.37%and RSD=1.519%.Aomisin showed a good relationship at the range of 0.011~1.76 mg/ml (r=0.9998).Regression Equation:y=10704x-24.666.The average recovery of syringin was 101.625%and RSD=1.307%.Deoxyschizandrin showed a good relationship at the range of 0.004~0.81mg/ml (r=1).Regression Equation:y=10601x-4.9829.The average recovery of syringin was 102.311% and RSD=0.824%.Conclusion:The method is simple,convenient and accurate,and can be used for content determination of Mixed ZiMu lipid classes in Wuweizi syrup.关键词
高效液相色谱法/五味子糖浆/五味子木脂素Key words
HPLC/Wuweizi syrup/Mixed ZiMu lipid classes分类
医药卫生引用本文复制引用
王杰姝,梁军,夏永刚,杨炳友,王秋红,张宇,匡海学..五味子糖浆中五味子木脂素类成分的含量测定[J].中医药学报,2014,(6):11-13,3.基金项目
国家科技重大专项重大新药创制（2012ZX09304005004）；黑龙江省博士后启动基金（ LBH－Q13158）；黑龙江中医药大学校科研基金 （）
