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复合活化剂制备稻壳活性炭影响因素及特性

刘斌 马叶 顾洁 周建斌

生物质化学工程Issue(4):35-39,5.
生物质化学工程Issue(4):35-39,5.DOI:10.3969/j.issn.1673-5854.2015.04.007

复合活化剂制备稻壳活性炭影响因素及特性

Preparation and Characterization of Activated Carbon from Rice Husk with Composite Activator

刘斌 1马叶 1顾洁 2周建斌2

作者信息

  • 1. 南京林业大学化学工程学院,江苏 南京 210037
  • 2. 南京林业大学材料科学与工程学院,江苏 南京 210037
  • 折叠

摘要

Abstract

A range of activated carbons were prepared from rice husk with ZnCl2-CuCl2 composite activator. The preparation conditions were optimized by orthogonal test using ZnCl2 concentration,CuCl2 concentration,activation temperature and activation time as effect factors. The adsorption properties of produced activated carbons were investigated. Rice husk-based activated carbon (RAC) was characterized by nitrogen adsorption-desorption isotherms and X-ray diffraction (XRD). Results indicated that rice husk could produce activated carbon with high surface area. The optimized conditions were as follows:5mol/L ZnCl2 ,0. 4 mol/L CuCl2 ,activation temperature 500℃,and activation time 2 h. The Iodine number,methylene blue value and BET surface area of the prepared activated carbon were 1 041 mg/g,188 mg/g and 1 924 m2/g,respectively.

关键词

活性炭/复合活化剂/稻壳/正交试验

Key words

activated carbon/composite activator/rice husk/orthogonal test

分类

化学化工

引用本文复制引用

刘斌,马叶,顾洁,周建斌..复合活化剂制备稻壳活性炭影响因素及特性[J].生物质化学工程,2015,(4):35-39,5.

基金项目

林业公益性行业科研专项项目(201304611) (201304611)

江苏省科技厅产学研联合创新资金-前瞻性联合研究项目( BY2014006-01) ( BY2014006-01)

林业科学技术推广项目([2014]40) ([2014]40)

生物质化学工程

OA北大核心

1673-5854

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