药学研究Issue(8)：453-454,2.
气相色谱法测定细辛脑注射液的含量
Determination of Asarone Injection by GC
吴永芹 1徐焕 2于立佐1
作者信息
- 1. 济宁市食品药品检验检测中心，山东 济宁 272000
- 2. 辰欣药业股份有限公司，山东 济宁 272073
- 折叠
摘要
Abstract
Objective To establish a gas chromatographic method for the determination of Asarone Injection. Methods The sample was analyzed on a TR - 1 capillary column(30 m × 0. 25 mm,0. 5 μm)with the column temperature at 160 ℃ . The detector was flame ionization detector(FID). Results There were good linearity between peak areas and con-centration of asarone within the range of 0. 100 4 ~ 5. 020 mg·mL - 1(r = 0. 999 6). The average recovery was 99. 1%(n =9)for asarone. Conclusion The method could be used for the determination of Asarone Injection. The gas chromatographic measurement was rapid,simple and reproducible and can be used as quality control for Asarone Injection.关键词
细辛脑注射液/气相色谱法/含量测定Key words
Asarone Injection/GC/Determination分类
医药卫生引用本文复制引用
吴永芹,徐焕,于立佐..气相色谱法测定细辛脑注射液的含量[J].药学研究,2015,(8):453-454,2.
