中医学报Issue(8)：1178-1180,3.DOI:10.16368/j.issn.1674-8999.2015.08.407
桃红四物汤中阿魏酸的含量测定
Determination of Ferulic Acid in Taohong Siwu Tang
王雁梅 1申现锋 1康美清 1史恒军2
作者信息
- 1. 漯河医学高等专科学校，河南 漯河462002
- 2. 第四军医大学唐都医院，陕西 西安710038
- 折叠
摘要
Abstract
Objective:To establish a determination method of ferulic acid in Taohong Siwu Tang. Methods:using Inertsil ODS-3 C18 col-umn(250 mm × 4. 6 mm,5 microns)as the stationary phase,methanol and water(including the volume fraction of 1% acetic acid)(45: 55,v/v)as mobile phase,flow rate of 1. 0 mL·min-1 . The detection wavelength was at 321 nm. Results:Ferulic acid had good line-arity in the range of 0. 6-180. 0 mg·L-1. The average recovery was 102. 65% and the repeatability(RSD)was 2. 23%. Conclusion:The developed method is rapid,sensitive and reproducible,which can be used to determine the contents of ferulic acid in Taohong Siwu Tang.关键词
桃红四物汤/阿魏酸/反相高效液相色谱法Key words
taohong siwu tang/ferulic acid/reversed-phase high-performance liquid chromatography分类
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王雁梅,申现锋,康美清,史恒军..桃红四物汤中阿魏酸的含量测定[J].中医学报,2015,(8):1178-1180,3.
