中国中医药信息杂志Issue(10)：94-96,3.DOI:10.3969/j.issn.1005-5304.2015.10.026
RP-HPLC测定藏药六味木香丸中木香烃内酯和去氢木香内酯含量
RP-HPLC Determination of Costunolide and Dehydrocostus Lactone in Tibetan Medicine Liuwei Muxiang Pill
焦正花 1刘效栓 1杨金草2
作者信息
- 1. 甘肃省中医院药学部，甘肃 兰州 730050
- 2. 甘南州食品药品检验所，甘肃 甘南 747000
- 折叠
摘要
Abstract
Objective To establish the method to analyze the contents of Costunolide and Dehydrocostus Lactone in Tibetan medicineLiuwei Muxiang Pill.Methods HPLC method was used; the XDB-C18 column (4.6 mm × 50 mm, 1.8μm) was adopted;the mobile phase was methanol- water (60∶40);the flow rate was 0.8 mL/min;UV detection was 225 nm.Results The linear range of Costunolide and Dehydrocostus Lactone was 0.235 5-1.413μg and 0.291 3-1.748μg. The average recoveries were 99.25% and 99.41%, respectively.Conclusion The method is accurate, reliable, stable and with good repeatability, which provides the basis for the quality evaluation of Tibetan medicineLiuwei Muxiang Pill.关键词
藏药六味木香丸/木香烃内酯/去氢木香内酯/高效液相色谱法Key words
Tibetan medicineLiuwei Muxiang Pill/Costunolide/Dehydrocostus Lactone/HPLC分类
医药卫生引用本文复制引用
焦正花,刘效栓,杨金草..RP-HPLC测定藏药六味木香丸中木香烃内酯和去氢木香内酯含量[J].中国中医药信息杂志,2015,(10):94-96,3.
