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X射线衍射仪固有角度刻度误差对点阵参数计算精确度影响的研究

徐晓明 苗伟 陶琨

物理学报Issue(13):1-6,6.
物理学报Issue(13):1-6,6.DOI:10.7498/aps.63.136001

X射线衍射仪固有角度刻度误差对点阵参数计算精确度影响的研究

Study on the effect of X-ray diffractometer inherent angle scale error on the precision of lattice parameter calculation

徐晓明 1苗伟 1陶琨1

作者信息

  • 1. 清华大学材料科学与工程研究院中心实验室北京 100084
  • 折叠

摘要

Abstract

This paper studies the effect of measuring angle error in X-ray powder diffractometer, which is caused by diffractome-ter inherent angle scale error resulting from mechanical manufacture, on the precision of calculated lattice parameter. It represents the theoretical limit of the consistency of the lattice parameters obtained by different diffractometers and laboratories. We use the calculated polysilicon diffraction patterns with random angle error to simulate the results mea-sured by many sets of diffractometers of some manufacturing precision, then calculate and analyze the lattice parameters by three methods.

关键词

X射线衍射仪/固有角度刻度误差/点阵参数/精确度

Key words

X-ray diffractometer/inherent scale error/lattice parameter/precision

引用本文复制引用

徐晓明,苗伟,陶琨..X射线衍射仪固有角度刻度误差对点阵参数计算精确度影响的研究[J].物理学报,2014,(13):1-6,6.

物理学报

OA北大核心CSCDCSTPCDSCI

1000-3290

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