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多弧离子镀负偏压对氮化钛薄膜的影响

宋沂泽 高原 董中新 张焱 彭凯 王成磊

表面技术2015,Vol.44Issue(11):1-6,28,7.
表面技术2015,Vol.44Issue(11):1-6,28,7.DOI:10.16490/j.cnki.issn.1001-3660.2015.11.001

多弧离子镀负偏压对氮化钛薄膜的影响

Influence of Negative Bias on TiN Film Deposited by Multi-arc Ion Plating

宋沂泽 1高原 2董中新 3张焱 4彭凯 4王成磊4

作者信息

  • 1. 广西信息材料重点实验室,广西 桂林541004
  • 2. 桂林电子科技大学材料学院, 广西桂林541004
  • 3. 桂林广陆数字测控股份有限公司, 广西桂林541004
  • 折叠

摘要

Abstract

Objective In order to improve the comprehensive performance of TiN coatings, the appropriate negative bias was in-vestigated. Methods TiN coatings were deposited with different negative bias voltage on the surface of 4Cr13 stainless steel, and the effect of negative bias voltage on the surface quality, microstructure, hardness, binding force and friction coefficient of the coa-tings was investigated. Results The results showed that negative bias voltage had an obvious influence on the surface quality of the TiN coating. When the negative bias voltage was 0 V, there were many droplets, larger particles and a few pits. With the increase of the bias voltage, the number and size of droplets on the film surface were reduced, and the coatings surface became smooth and more compact. TiN films deposited at different bias voltage all showed preferred orientation in (111) crystal plane, but with the increase of bias voltage, the preferred orientation gradually diminished, when the bias voltage was 400 V, the peak value of the film on the (220) crystal plane was gradually strengthened. When the bias voltage changed between 0 V and 400 V, the hardness, fording force and abrasion resistance of coatings first increased and then decreased. When the bias voltage was 300 V, the biggest hardness and fording force reached 2650HV and 58 N, respectively;The friction coefficient and abrasion loss were 0. 48 and 0. 1065 mm3 , respec-tively. Conclusion Applying proper negative bias voltage could improve the comprehensive properties of coatings, such as hardness, fording force and abrasion resistance. When the bias voltage was 300 V, the TiN film deposited showed the best properties.

关键词

多弧离子镀/氮化钛/负偏压/耐磨性/结合力/硬度

Key words

MAIP/TiN/negative bias voltage/wear resistance/fording force/hardness

分类

矿业与冶金

引用本文复制引用

宋沂泽,高原,董中新,张焱,彭凯,王成磊..多弧离子镀负偏压对氮化钛薄膜的影响[J].表面技术,2015,44(11):1-6,28,7.

基金项目

国家自然科学基金资助项目(51264007) (51264007)

国家自然科学基金青年基金(51201043) (51201043)

广西科学研究与技术开发科技攻关计划(12118020-2-2-1) (12118020-2-2-1)

广西信息材料重点实验室(桂林电子科技大学)资助(1210908-10-Z) (桂林电子科技大学)

桂林电子科技大学-桂林电科院研究生联合培养基地专项经费资助(20121225-10-Z ()

20121225-03-Z) Supported by the National Natural Science Foundation of China (51264007), the National Natural Science Foundation of China (51201043 ),Guangxi Development of Science and Technology Research(12118020-2-2-1), Guangxi Key Laboratory of Information Materials (Guilin University of Electronic Tech-nology) (1210908-10-Z), and Guilin University of Electronic Technology-Electrical Science Graduate Student of Joint Training Base under Special Funding (20121225-10-Z, 20121225-03-Z) (51264007)

表面技术

OA北大核心CSCDCSTPCD

1001-3660

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