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HPCL法测定乳痛软坚片中橙皮苷含量的研究

夏英

中医药导报Issue(7):91-92,2.
中医药导报Issue(7):91-92,2.

HPCL法测定乳痛软坚片中橙皮苷含量的研究

Determination of Hesperidin in Breast Pain Softening Hardness Tablets by HPLC

夏英1

作者信息

  • 1. 湖南中医药大学第一附属医院,湖南 长沙 410007
  • 折叠

摘要

Abstract

Objective: To establish a method to determine the content of Hesperidin in Breast Pain Softening Hardness Tablets by HPLC. Methods: The HPLC method was applied and Diamonsil Kromasil-C 18 was used; Methanol - water(20∶80) was used as mobile phase; detective wave was 284 nm; flow rate was 1.0 mL/min; column temperature was 30 ℃. Results: The linear range of Hesperidin was 32-800μg/μL, r=0.9998, The average recovery of ephedrine hydrochloride was 98.04%,RSD%=1.6%. Conclusion: This method is high resolution, simple and quick, with stable result. It can be used for quality control of Breast Pain Softening Hardness Tablets.

关键词

HPLC法/乳痛软坚片/橙皮苷/含量测定

Key words

HPLC/Breast Pain Softening Hardness Tablets/Hesperidin/Determination of conten

分类

医药卫生

引用本文复制引用

夏英..HPCL法测定乳痛软坚片中橙皮苷含量的研究[J].中医药导报,2013,(7):91-92,2.

中医药导报

OACSTPCD

1672-951X

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