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HPLC 法测定更年安胶囊含量的方法研究

历娜 尚金燕 姜爱霞

药学研究Issue(11):640-641,2.
药学研究Issue(11):640-641,2.

HPLC 法测定更年安胶囊含量的方法研究

Study on the determination of Gengnian′an Capsules by HPLC

历娜 1尚金燕 1姜爱霞1

作者信息

  • 1. 山东药品食品职业学院,山东 威海 264210
  • 折叠

摘要

Abstract

Objective To establish an HPLC method for the determination of Gengnian′an Capsules. Methods Using the Dalian Elite C18 column,acetonitrile,water and glacial acetic acid(60:40:1),the flow rate was 1. 0 mL·min - 1 ,the de-tection wavelength was 437 nm and the injection volume was 10 μL. Results The linear range was good within the concen-tration of 0. 040 ~ 0. 600 mg·mL - 1 ,r = 0. 993 9,RSD of the reproducibility test was 1. 35% ,the average recovery was 96. 67%(RSD = 1. 33% ). Conclusion This method was sensitive,simple,accurate and reproducible,and could effectively control the content of Gengnian′an Capsules.

关键词

更年安胶囊/高效液相色谱法/含量

Key words

Gengnian′an Capsules/HPLC/Content

分类

医药卫生

引用本文复制引用

历娜,尚金燕,姜爱霞..HPLC 法测定更年安胶囊含量的方法研究[J].药学研究,2015,(11):640-641,2.

药学研究

2095-5375

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