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养心生脉颗粒挥发性成分的 GC -MS 分析

王翠竹 陈金鸾 张仲毅 张浩 张楠淇 李平亚

特产研究Issue(3):58-60,3.
特产研究Issue(3):58-60,3.

养心生脉颗粒挥发性成分的 GC -MS 分析

Analysis of the Volatile Constituents from Yangxinshengmai Granules with GC -MS

王翠竹 1陈金鸾 1张仲毅 2张浩 1张楠淇 1李平亚1

作者信息

  • 1. 吉林大学药学院,长春 130021
  • 2. 山海关药业有限责任公司,河北 秦皇岛 066000
  • 折叠

摘要

Abstract

GC-MS (gas chromatography-mass spectrometry ) was used to analyze the volatile oil components in Yangxinshengmai Granule to provide theoretical basis for determination of its chemical constituents and quality control .The volatile oil of Yangxinshengmai Granule was ex-tracted with steam distillation method ,the chemical compositions were separated by GC capillary column chromatography and identified by mass spectrometry ,and the relative content of constituents were determined by area normalization method .31 compounds were detected and 25 com-pounds of them were identified .And the compounds with higher relative contents were Palmitic acid (49.25% ) ,Linoleic acid (20.94% ) ,9-trans-Octadecenoic acid(3.58% ) ,and Stearic acid(3.28% ) ,respectively .The main components in volatile oil of Yangxinshengmai Granule were alkanes ,esters and fatty acid ,etc .

关键词

养心生脉颗粒/挥发性成分/气相色谱-质谱联用/化学成分

Key words

Yangxinshengmai granule/volatile constituents/Gas chromatography -mass spectrometry/chemical constituent

分类

医药卫生

引用本文复制引用

王翠竹,陈金鸾,张仲毅,张浩,张楠淇,李平亚..养心生脉颗粒挥发性成分的 GC -MS 分析[J].特产研究,2015,(3):58-60,3.

基金项目

吉林大学研究生创新研究计划项目 ()

特产研究

OACSTPCD

1001-4721

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