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六方氮化硼纳米片的制备

李军奇 周健 郝红娟 崔明明

陕西科技大学学报(自然科学版)Issue(6):40-43,4.
陕西科技大学学报(自然科学版)Issue(6):40-43,4.

六方氮化硼纳米片的制备

Preparation of hexagonal boron nitride nanosheet

李军奇 1周健 1郝红娟 1崔明明1

作者信息

  • 1. 陕西科技大学材料科学与工程学院,陕西西安 710021
  • 折叠

摘要

Abstract

A certain layer ,specific surface area and large pieces of boron nitride nanosheets were successfully fabricated through two simple methods .The first one is fabricated through pyroreaction by using H3BO3 as the source of the boron and H2 NCONH2 as the source of the nitrid ,the second method was successfully fabricated through chemical exfoliation by using the boron nitride powder .The crystallinity ,morphology and size of the sample were charac‐terized by X‐ray powder diffraction (XRD) ,Raman ,scanning electron microscope (SEM ) and transmission electron microscopy (TEM) .The results showed that the crystalline of bo‐ron nitride nanosheets is poor ,the diameter is about 2 μm and the thickness is about 2 nm , which was fabricated by pyroreaction .The boron nitride nanosheets has been successfully fabricated by chemical exfoliation w hich has high crystalline , the diameter is 80 nm ,the thickness is about 4~5 nm .

关键词

六方氮化硼/高温反应/化学剥离法

Key words

hexagonal boron nitride/pyroreaction/chemical exfoliation

分类

化学

引用本文复制引用

李军奇,周健,郝红娟,崔明明..六方氮化硼纳米片的制备[J].陕西科技大学学报(自然科学版),2015,(6):40-43,4.

基金项目

陕西科技大学学术骨干培育计划项目 ()

陕西科技大学学报(自然科学版)

OACSTPCD

2096-398X

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