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还原法制备银纳米粒子/氧化石墨烯的纳米复合物及其表征

丁永萍 何茂伟 郭玉玮

信阳师范学院学报(自然科学版)Issue(3):395-398,4.
信阳师范学院学报(自然科学版)Issue(3):395-398,4.DOI:10.3969/j.issn.1003-0972.2013.03.022

还原法制备银纳米粒子/氧化石墨烯的纳米复合物及其表征

Synthesis and Characterization of Silver Nanoparticles/Oxidation Graphene Nanocomposites by the Reduction Method

丁永萍 1何茂伟 2郭玉玮1

作者信息

  • 1. 包头师范学院 化学学院,内蒙古 包头 014030
  • 2. 山东源根石油化工有限公司,山东 济宁 272000
  • 折叠

摘要

Abstract

Polyethyleneimine /graphene(PEI/GO) nanocomposites were prepared by the green reduction method and the feature that amino-groups are rich in PEI chain of the macromolecular polymer .Then, the AgNPs /PEI/GO complexes were prepared by immobilizing silver nanoparticles on the surface of PEI /GO nanocomposites utilizing the re-ducing effect of amino-group on silver ion and the protection effect of silver nanoparticles .The influences of reaction time and concentration of silver ions on the prepared silver nanocomposites were studied .The prepared AgNPs /PEI/GO complexes were characterized using infrared spectroscopy , UV spectra, XRD, TEM, and other means.The char-acterization results showed that PEI was successfully modified to GO surface , Ag + was reduced using green and clean technology and immobilized on GO surface .The AgNPs/PEI/GO nanocomposites have good electric conductive proper -ties and perfect crystal phase .

关键词

石墨烯/聚乙烯亚胺/银纳米粒子复合物/绿色还原法

Key words

graphene/polyethyleneimine/silver nanoparticles composites/green reduction method

分类

化学化工

引用本文复制引用

丁永萍,何茂伟,郭玉玮..还原法制备银纳米粒子/氧化石墨烯的纳米复合物及其表征[J].信阳师范学院学报(自然科学版),2013,(3):395-398,4.

基金项目

内蒙古自治区教育厅高校科研项目(NJ06002);校内青年科研资助项目 ()

信阳师范学院学报(自然科学版)

OA北大核心CSTPCD

1003-0972

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