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连续滴定法测定硅氟酸电解液中硅氟酸和铅

谭凤 张桂兵

云南化工Issue(5):44-47,4.
云南化工Issue(5):44-47,4.DOI:10.3969/j.issn.1004-275X.2015.05.011

连续滴定法测定硅氟酸电解液中硅氟酸和铅

Determination of Silicon Fluoride Acid and Lead in Silicon Fluoride Acid Electrolyte by Continuous Titration

谭凤 1张桂兵1

作者信息

  • 1. 云南锡业股份公司,云南 个旧 661000
  • 折叠

摘要

Abstract

The saturated potassium sulfate is added in the electrolyte leading to the formation of pre-cipitation of silicon fluoride acid and lead separated from other elements.After the silicon fluoride acid was titrated with sodium hydroxide solution,the lead was tritrated with EDTA.The recovery rate of the silicon is 97.9% to 101.3%,the recovery of lead is 97% to 102.07%,the method is simple,accurate and fast,and can meet the requirements of production.

关键词

电解液/硅氟酸//连续滴定法

Key words

electrolyte/silicon fluoride acid/lead/continuous titration

分类

化学化工

引用本文复制引用

谭凤,张桂兵..连续滴定法测定硅氟酸电解液中硅氟酸和铅[J].云南化工,2015,(5):44-47,4.

云南化工

1004-275X

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