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硬脂酸三乙醇胺酯的分析

王明权

印染助剂2015,Vol.32Issue(9):24-27,4.
印染助剂2015,Vol.32Issue(9):24-27,4.

硬脂酸三乙醇胺酯的分析

Analysis of triethanolamine esters of stearic acid

王明权1

作者信息

  • 1. 南京化工职业技术学院,江苏南京 210048
  • 折叠

摘要

Abstract

With the mixture of V(chloroform):V(methanol)=25:1 as eluent, three fractions of stearic acid triethanolamine ester were obtained by silica gel column chromatography separation, and analyzed qualitatively by high efficiency liquid chromatography (HPLC), infra-red spectrum (IR) and mass spectra (MS). The results in?dicated that the three fractions were triesteramine, diesteramine and monoesteramine respectively. With the corresponding standard curve of the three high purity components of triesteramine, diesteramine and monoes?teramine, combined with the results of HPLC and column chromatography separation, the HPLC was a conve?nient, quick and exact method for quantitative analysis of triethanolamine esters of stearic acid.

关键词

硬脂酸三乙醇胺酯/馏分/定性分析/定量分析

Key words

triethanolamine esters of stearic acid/fraction/qualitative analysis/quantitative analysis

分类

化学化工

引用本文复制引用

王明权..硬脂酸三乙醇胺酯的分析[J].印染助剂,2015,32(9):24-27,4.

印染助剂

OA北大核心CSTPCD

1004-0439

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