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气相色谱法测定地塞米松磷酸钠注射液中丙三醇含量

耿倩 赵云鹏 王建明

医学信息Issue(17):596-597,2.
医学信息Issue(17):596-597,2.

气相色谱法测定地塞米松磷酸钠注射液中丙三醇含量

Determination the Assay of Glycerol in Dexamethasone Sodium Phosphate Injection by GC

耿倩 1赵云鹏 1王建明1

作者信息

  • 1. 石药集团欧意药业有限公司,河北 石家庄 050051
  • 折叠

摘要

Abstract

To establish a method for determination the assay of glycerin in Dexamethasone Sodium Phosphate Injection, use GC with column of HP-1, nitrogen as the carrier gas, and FID as the detector, use external standard method to calculate the assay of glycerin. Peak area and concentration presents good linearity in experimental range, the correlation coef icient is 0.999, the average recovery is 97%(n=9),RSD is 0.8%.The method has a good specificity, reproducibility, accurancy and high sensitivity, can use to determination the assay of glycerin in Dexamethasone Sodium Phosphate Injection.

关键词

气相色谱法/地塞米松磷酸钠注射液/丙三醇/含量

Key words

GC/Dexamethasone Sodium Phosphate Injection/Glycerol/Assay

引用本文复制引用

耿倩,赵云鹏,王建明..气相色谱法测定地塞米松磷酸钠注射液中丙三醇含量[J].医学信息,2013,(17):596-597,2.

医学信息

1006-1959

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