中国中医药信息杂志Issue(8)：52-53,54,3.DOI:10.3969/j.issn.1005-5304.2013.08.018
气相色谱法测定克疣纳米乳中冰片和薄荷脑含量
GC Determination of Synthetic Borneol and Menthol in Keyou Nanoemulsion
摘要
Abstract
Objective To establish the determination method synthetic borneol and menthol in Keyou nanoemulsion. Methods HP-5 quartz capillary column (30 m×320 µm×0.25 µm) was used with nitrogen as the carrier gas, and FID as the detector. The temperature of the entrance of the capillary vessel column was at 230 ℃. Results Synthetic borneol and menthol in Keyou nanoemulsion were separated well. The calibration curves of synthetic borneol was obtained with good linear relationship within the range of 0.337-1.685 µg (r 2=0.998 2), the average recovery was 97.5%. The calibration curves of menthol was also obtained with a good linear relationship within the range of 0.234-1.17 µg (r 2=0.997 4), the average recovery was 97.0%. Conclusion The methord is simple and accurate. It can be used to control the quality of Keyou nanoemulsion.关键词
克疣纳米乳/冰片/薄荷脑/气相色谱法Key words
Keyou nanoemulsion/synthetic borneol/menthol/GC分类
医药卫生引用本文复制引用
樊静静,袁玉霞,尹香阁,赵文龙,贾永艳..气相色谱法测定克疣纳米乳中冰片和薄荷脑含量[J].中国中医药信息杂志,2013,(8):52-53,54,3.基金项目
郑州市科技攻关项目(0910SGYS33390-2) （0910SGYS33390-2）
